Westfälische Wilhelms-Universität Münster: Forschungsbericht 2003-2004 - Institut für Materialphysik

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Institut für Materialphysik

Tel. (0251) 83-33571
Fax: (0251) 83-38346
e-mail: epped@uni-muenster.de
www: uni-muenster.de/Physik/MP/
Wilhelm-Klemm-Str. 10
48149 Münster
Direktor: Prof. Dr. Helmut Mehrer

Forschungsschwerpunkte 2003 - 2004  
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Strengthening and Nanostructure of Metals and Alloys
The detrimental effects of precipitate free zones on the yield strength of polycrystals of the commercial nickel-base superalloy NIMONIC PE16, which is strengthened by nano-scale precipitates of the g'-phase

 
The dispersion of nano-scale g'-precipitates and the width w of g'-precipitate free zones (PFZ) along grain boundaries have been varied systematically for the commercial nickel-base superalloy NIMONIC PE16. This material serves as a model system in a general study of the effects of PFZs. The yield strength sy was found to decrease as w increases provided w exceeds a minimum value. The maximum observed decrease of sy amounts to 25%. The technical relevance of this effect is evident. The dislocation processes in the PFZs have been studied by stretching thin foils inside a transmission electron microscope and observing the glide of dislocations under full load. Softening due to PFZs is mainly caused by the ease with which dislocations are created in the PFZs; this leads to concentrated slip. Attempts to eliminate the detrimental effects of PFZs by double aging treatments failed.

Drittmittelgeber:

Deutsche Forschungsgemeinschaft

Beteiligte Wissenschaftler:

Dr. D. Baither, Dr. T. Krol, P.D. Dr. V. Mohles, Prof. a. D. Dr. E. Nembach (Leiter), P.D. Dr. J. Pesicka, Dipl.-Phys. V. Vovk

Veröffentlichungen:

Krol, T., D. Baither, E. Nembach:
Quantification of the detrimental effects of precipitate free zones on the yield strength of a superalloy
Scripta Mater., 48 (2003), 1189

Baither, D., T. Krol, E. Nembach:
In-situ transmission electron microscopy study of dislocation processes at precipitate-free zones in a g'-strengthened superalloy
Phil. Mag., 83 (2003), 4011

Baither, D., T. Krol, E. Nembach:
Dislocation processes in precipitate free zones in NIMONIC PE16 studied by TEM
Mat. Sci. Eng. A, 387-389 (2004), 163

Krol, T., D. Baither, E. Nembach:
Softening of the superalloy NIMONIC PE16 by precipitate free zones along grain boundaries
Mat. Sci. Eng. A, 387-389 (2004), 214

Krol, T., D. Baither, E. Nembach:
The formation of precipitate free zones along grain boundaries in a superalloy and the ensuing effects on its plastic deformation
Acta Mater., 52 (2004), 2095

Nembach, E., J. Pesicka, V. Mohles, D. Baither, V. Vovk, T. Krol:
The effects of a second aging treatment on the yield strength of g'-hardened NIMONIC PE16- polycrystals having g'-precipitate free zones
Acta Mater., 53 (2005) 2485

Baither, D., V. Mohles, E. Nembach:
In situ transmission electron microscopy tensile tests of a peak- to overaged g'-strengthened nickel base alloy
Journal of Materials Research, in press

 

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