Equipment Laboratory
Equipment Laboratory
Seven hoods and one hood suitable for synthesis with inert gas extinguishing system are available
Organic Analysis
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MaXis 3G UHR-QTOF-MS, Bruker, ultra high resolution quadrupole time-of-flight mass spectrometer, resolution 1 ppm, MS/MS and pseudo MS3 experiments, aquisition rate 50 Hz, electro spray ionization (ESI) source for coupling with LC, atmospheric pressure laser ionization (APLI) source for coupling with GC or LC, potentially feasible atmospheric pressure chemical ionization (APCI) source for coupling with GC or LC and atmospheric pressure photo ionization (APPI) source for coupling with GC or LC |
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GC-2010Plus (GC), Shimadzu, two split/splittless injectors SPL-2010plus, AOC20i autosampler, sample tray for 98 2 ml vials, two flowlines, flame ionization detector (FID), GCsolution software |
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Prominence UFLCXR (LC), Shimadzu, ultra performance liquid chromatography, 2 LC-20ADXR double plunger pumps, semi micro mixer, automatic rinsing kit, DGU-20A3 online degasser, SIL-20AXR autosampler, CTO-20AC column oven, SPD-20AV UV-detector, CBM-20A system controller, LC solution software |
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GCMS-QP-2010Plus EI/CI/NCI-System (GC-MS), Shimadzu, Optic3-PTV injector (split/splitless, programmed temperature vaporizer, on-column-injection, thermodesorption, difficult matrix introduction, rapid large volume injection) with LN2 cooling, additional split/splittless injector, Zoex modulator GCxGC with compressor cooling, Combi PAL Autosampler (liquid and headspace injection, automatized solid phase micro extraction, Peltier cooler 4°C to 70°C), simultaneous SIM and SCAN, GCMSsolution software, GC Image software, Cycle Composer software |
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SpeedExtractor E-916, Büchi, solvent extractor, parallel extraction of max. 6 samples, 12 stainless steel cells 10 ml and 6 stainless steel cells 40 ml, 250 ml collection vessels, possibility to use Büchi Syncore Analyst R-12 evaporation vessels as collection vessels |
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Syncore Analyst R-12, Büchi, parallel evaporation of 12 samples (120 ml) with residual volume cooling (0,3 ml), condenser, flushback module, solid phase extraction module, separate vacuum pump V-700 with controller V-855, rotation speed controlled |
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Hei-Vap Precision ML/HB/G3B, Heidolph, rotary evaporator, Rotavac vario control vacuum pump, AUTOaccurate temperature sensor |
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Vapotherm Basis Mobil I, Barkey, parallel evaporation of 10 samples (10 ml), max. set temperature 120 °C, viewing window (glass), turn over device, nitrogen gassing |
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Inorganic Analysis |
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ICP-OES SpectroFlame-EOP, SPECTRO Analytical Instruments, inductively coupled plasma optical emission spectrometry, Smart Analyzer 2.25 software |
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761 Compact IC, Metrohm, ion chromatography, 753 supressor module, 813 Compact autosampler (36 samples), 761 Compact IC 1.1 software |
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Hydraulic and Soil Mechanic Laboratory |
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Pulverisette 7, Fritsch, planetary micro mill, 2 grinding beakers 12 ml and 45 ml stainless steel, (agate), silicium nitride each |
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Other Equipment |
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Genesys 10UV, Thermo, UV Vis spectrophotometer, Xenon lamp, 190 - 1100 nm |
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672 Titroprocessor and 655 Dosimat, Metrohm, for titration, up to 5 ml and 10 ml |
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ItaChrom EA 101, Merck, isotachophoresis, separation of ions |
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Alpha 1-4 LDplus, Christ, freezing dry machine, 0.51 kW, ice condenser temperature -60 °C, ice condenser chamber 6.5 l, 5 shelves į 360 mm diameter, 18 connections for round bottom flasks |
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Centrifuge MR22i, Jouan (Thermo Electron), 20 to 17,000 x g (36,668 x g), 4 x Ø 44 / 56 mm, 6 x Ø 24 mm with 6 x high strenght glas tubes 30 mL usable to 12,100 x g |
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Biofuge R15, Heraeus, max. 20,000 x g, 24 x Ø 10 mm |
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SM 30 A, Edmund Bühler, shaker, orbital, up to 300 rpm |
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Milli-Q Integral 5, Millipore, ultrapure water purification system, TOC Analyzer, Q-POD Dispenser, PE Reservoir 30 l, typical electrical conductivity 0,055 µS/cm, typical TOC-concentration 3 ppb |
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EURO 10 plus, SG Wasseraufbereitung und Regenerierstation GmbH, reverse osmosis system with EI-Ion electro-deionization, EURO reservoir 80 l with level measurement and integrated booster pump, typical electrical conductivity 0,056 µS/cm |
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