Under normal circumstances
we use an ordinary Schlenkline to handle O2 and H2O
one of our gloveboxes
running with Argon.
Our Infrared spectrometer
... mass spectrometer are
attached to the high-vacuum line.
As our standard reactants are sensitive to hydrolysis, we use
Schlenklines which are evacuated up to 1·10-3
mbar. As inertgas argon or nitrogen are in use.
with Si and Sn:
Some of our reactants or products are very volatile (e.g. b.p. of F3CBr
-56°C) so we need to work in a vacuum-line or modified
For meassurements we need either single crystals which are fixed
directly onto the goniometerhead of X-Ray diffratometers or we have to
grow a single crystal from low-melting liquids by application of